Noble metal impregnation has resulted in the inclusion of metal nanostructures within the SBA-15 mesoporous silica hexagonal pores (from nanoclusters to nanowires). A bright-field transmission electron microscopy three-dimensional reconstruction is proposed to analyze the localization of nanostructures within the pores of mesoporous nanotemplates. The method allows corroboration whether the nanostructures are synthesized inside the pores or they are synthesized alternatively on the nanotemplate aggregates exterior surface.
Published in Electrochemical and Solid-State Letters, Volume 7, Issue 7, 2004, pages J17-J19.
©Electrochemical Society 2004, The Electrochemical Society.
© The Electrochemical Society, Inc. [year]. All rights reserved. Except as provided under U.S. copyright law, this work may not be reproduced, resold, distributed, or modified without the express permission of The Electrochemical Society (ECS). The archival version of this work was published in Electrochemical and Solid-State Letters.
Publisher’s Version: http://dx.doi.org/10.1149/1.1724827
Arbiol, J., Rossinyol, E., Cabot, A., Peiro, F., Cornet, A., Morante, J. R., Chen, F., & Liu, M. (2004). Nobel Metal Nanostructures Synthesized inside Mesoporous Nanotemplate Pores. Electrochemical and Solid-State Letters, 7 (7), J17 – J19. http://dx.doi.org/10.1149/1.1724827